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Calibration is necessary in order to find the relation of the difference in position of the keel (the "signal") and the difference in weight. ) by rocking the ship. This up and down movement of the keel may be big enough to completely mask the small displacement which is to be measured. In this case the weight of the captain is below the "limit of detection" of this ingeneous method. Elimination of the blank portion is necessary because the bottom of the basin may be uneven. This can be controlled by measuring the depth of the water.

40 V, ramenant ainsi tous les potentiels à une origine qui sera l'électrode normale à hydrogène dans l'eau. Mais l'utilisation de cette méthode a présenté ici des difficultés. Il faut d'abord s'assurer que le couple du ferrocene répond bien dans les mélanges acide sulfurique-eau aux conditions demandées : propriétés oxydo-réductrices indépendantes du solvant. Il est alors indispensable de le comparer à une autre référence de nature très différente. Par ailleurs son potentiel est trop bas et la solubilité trop faible en milieu concentré pour qu'on puisse l'utiliser autrement que dans les milieux riches en eau.

Stephen and P. C. Uden, Chem. , 41 (1971). E. Bayer, H. Müller and R. E. Sievers, Anal. , 43, 2012 (1971). R. Belcher, C. R. Jenkins, W. I. Stephen and P. C. Uden, Talanta, 17, 455 (1970). R. Barrati, R. Belcher, W. I. Stephen and P. C. Uden, Anal. Chim. Acta, 58, 107 (1971). R. Barrait, R. Belcher, W. I. Stephen and P. C. Uden, Anal. Chim. Acta, 59, 59 (1972). R. Belcher and W. I. Stephen, unpublished work. A. E. Jenkins and J. R. Majer, Mass Spectrometry, p. 253, Butterworths, London (1968). A.

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